IBX: 2-Iodoxybenzoic acid

Alcohol 139:

Flash Chromatography:
A rapid form of column chromatography in which the separation of molecules is air pressure driven. Silica gel is packed into a column of 6”-10.” As with other columns, the top of the column should not be allowed to run dry. It is a very fast (5-10 minutes) and economical method of purification.

Source: http://www.saiadsorbents.com/flash.htm
COSY:
One of the several types of two-dimensional NMR Spectroscopy used todetermine the connectivity of a molecule by identifying which protons are spin-spin coupled. The two-dimensional data is generated from a series of one-dimensional experiments. In each experiment there is a sequence of radio frequency pulses with delay periods in between. Throughout some of the delays, the nuclear spins rotate for a determined length of time known as evolution time. Changing the evolution time in successive one-dimensional experiments accrues the two-dimensional data
.
Source: http://en.wikipedia.org/wiki/Correlation_spectroscopy
http://www2.hmc.edu/www_common/chemistry/nmr/page9.htm

HMQC (Heteronuclear Multiple Quantum Coherence):
A two-dimensional inverse H, C technique that determines the heteroatom (usually carbon) to hydrogen connectivity. It is selective for direct C-H coupling.
Source: http://www.chemistry.msu.edu/facilities/nmr/HMQC.html
HMBC (Heteronuclear Multiple Bond Coherence):
Another two-dimensional inverse H, C technique allowing for determination of connectivity, but selective for longer range couplings (2-4 bond coupling).
Source: http://www.chemistry.msu.edu/facilities/nmr/HMQC.html

Grignard 137: